Graphical Plot of Background vs. Z-bar

EPMA Probe

Graphical Plot of Background vs. Z-bar

To tell the program which MAN backgrounds you want to use on which channels, click the MAN Fits under the Analytical menu. The program will load the standard count data and graphically plot the acquired MAN background samples using a default assignment. After selecting or deselecting (hold down the <ctrl> key while clicking) standards in the standard list box click the Update Fit button to save the changes. The program will then calculate and display the updated fit. The intercept, slope and curvature coefficients and the average relative deviation in percent is also displayed on the graph. You should avoid using samples which contain the channel element or produce an interference. These samples will show up as high points on the graph.

Note that the default selection of MAN standards by Probe for EPMA is somewhat intelligent; if the standard database composition for the standard contains more than 0.01 weight percent of the element in question, then the program will not assign that standard in the initial plot. Of course, the user can still specify the standard explicitly by clicking it in, but remember, if the element is present then you are not actually measuring the background for that element. The "force linear fit" option can be used when you feel that the program is over-fitting the data.

You can assign the MAN fits as soon as you finish collecting data for the backgrounds, or just before you begin your first analysis. You can change the MAN assignments you have made at any time. If additional MAN backgrounds are necessary, add them to the run and acquire the additional data.